6th WCSET-2017 at Indonesia
Technical Session 6:
Title:
Characterization and Contrast Enhancement of ZnO
Nanoparticles Dispersed 6OCB Liquid Crystalline
p-n-hexyloxy cyanobiphenyl Compound
Authors: P
Jayaprada, B T P Madhav, P Pardhasaradhi, G Giridhar, T
E Divakar, R K N R Manepalli
Abstract: In the present paper
synthesis and characterizationare carried on ZnO
nanoparticles dispersed in Liquid Crystalline
p-n-hexyloxy cyanobiphenyl (6OCB) compound. We have ZnO
reported nanoparticles are synthesized by Autoclave
method which is having a broad range of applications and
dramatically effects the birefringence properties of
6OCB when dispersion with low concentration. The
Polarizing Optical Microscopy (POM) technique is used to
measure the phase transition temperatures along with
texture identification. Further characterization is
carried out by various spectroscopic techniques like
X-ray Diffraction Studies (XRD), Scanning Electron
Microscopy (SEM), and Ultra Violet Visible (UV-Vis)
spectroscopy. Textural determinations of the synthesized
compounds are recorded by using POM connected with a hot
stage and camera. The results showed that the dispersion
of ZnO and in 6OCB exhibit nematic phase as same as the
pure 6OCB with slightly reduced clearing temperature as
expected. Image processing based contrast enhancement
for better visibility and for the identification of
liquid crystalline phases also performed with linear
stretching method.
Keywords: Synthesis, POM, DSC,
Nano-dispersion, XRD, SEM and UV
Pages:
176-180